| Título: | Development of a harmonised method for the profiling of amphetamines: I. Synthesis of standards and compilation of analytical data |
| Autores: |
Aalberg, Laura Andersson, Kjell Bertler, Christina Borén, Hans Cole, Michael D. Dahlén, Johan Finnon, Yvonne Huizer, Henk Jalava, Kaisa Kaa, Elisabet Lock, Eric Lopes, Alvaro Poortman-van der Meer, Anneke Sippola, Erkki |
| Fecha: |
2010-05-05 2010-05-05 2005-05 |
| Publicador: | Anglia Ruskin University |
| Fuente: |
 |
| Tipo: | Article |
| Tema: |
amphetamine profiling impurities synthesis infrared spectroscopy gas chromatography–mass spectrometry 1H NMR 13C NMR UV |
| Descripción: | Reference material was synthesised for 21 substances that are frequently present as synthetic impurities, i.e. by-products, in illicitly produced amphetamine. Each of these substances is a typical by-product for at least one of the three approaches most often used to synthesise amphetamine, namely, the Leuckart, the reductive amination of benzyl methyl ketone, and the nitrostyrene routes. A large body of data on the substances was recorded, including the following: mass spectra, ultraviolet spectra, Fourier transform infrared spectra, infrared spectra in gas phase, and 1H NMR and 13C NMR spectra. |
| Idioma: | Inglés |
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